10.3390\/cryst11040334<\/a><\/p>\nAuthors:<\/h4>\n
H.N. Sumedha, Mabkhoot Alsaiari, Mohammed Jalalah, M. Shashank, Fahad A. Alharthi, Naushad Ahmad, Jari S. Algethami, Vishwanth Vishwanth, G. Nagaraju<\/p>\n
Abstract:<\/h4>\n
We report a facile synthesis of \u03b2-SnWO4 nanoparticles via a microwave heat treatment using SnCl2 and H2WO4 in the presence of tamarind seed powder. An X-ray diffraction analysis confirmed a crystalline nature revealing a cubic structure of \u03b2-SnWO4 nanoparticles. The morphological features were visualized using a scanning electron microscope that exhibited homogenously distributed clusters of nanoparticles, which were further confirmed using a transmission electron microscope. The micrographs also displayed some porosity. Energy dispersive X-ray spectroscopy confirmed the elemental contents such as tin, oxygen and tungsten in the same stoichiometric ratio as expected by the respective empirical formula. A high-resolution transmission electron microscope was used to find the d-spacing, which was ultimately used to analyze the structural parameters. The spectrum obtained using Fourier transform infrared spectroscopy illuminated different stretching vibrations. Additionally, a Barrett\u2013Joyner\u2013Halenda analysis was carried out to investigate the N2 adsorption-desorption isotherm as well as to govern the pore size distribution. Cyclic voltammetry measurements were implemented to analyze the ongoing electrode reactions throughout the charge\/discharge for the \u03b2-SnWO4 nanostructures. The galvanometric charge\/discharge curves for \u03b2-SnWO4 are also discussed. A high specific capacitance (600 mAhg\u20131 at 0.1 C) and excellent columbic efficiency (~100%) were achieved.<\/p>\n","protected":false},"excerpt":{"rendered":"
DOI: 10.3390\/cryst11040334 Authors: H.N. Sumedha, Mabkhoot Alsaiari, Mohammed Jalalah, M. Shashank, Fahad A. Alharthi, Naushad Ahmad, Jari S. Algethami, Vishwanth Vishwanth, G. Nagaraju Abstract: We report a facile synthesis of \u03b2-SnWO4 nanoparticles via a microwave heat treatment using SnCl2 and H2WO4 in the presence of tamarind seed powder. An X-ray diffraction analysis confirmed a crystalline […]<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[2],"tags":[],"class_list":["post-45","post","type-post","status-publish","format-standard","hentry","category-bcs-800-battery-cycler"],"_links":{"self":[{"href":"https:\/\/citations.tools.bio-logic.fr\/index.php?rest_route=\/wp\/v2\/posts\/45","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/citations.tools.bio-logic.fr\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/citations.tools.bio-logic.fr\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/citations.tools.bio-logic.fr\/index.php?rest_route=\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/citations.tools.bio-logic.fr\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=45"}],"version-history":[{"count":0,"href":"https:\/\/citations.tools.bio-logic.fr\/index.php?rest_route=\/wp\/v2\/posts\/45\/revisions"}],"wp:attachment":[{"href":"https:\/\/citations.tools.bio-logic.fr\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=45"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/citations.tools.bio-logic.fr\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=45"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/citations.tools.bio-logic.fr\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=45"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}